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Koller, Jürgen, McElwee-White, Lisa, Abboud, Khalil A. (2007) An N-bridged tritungsten compound for the chemical vapor deposition of WN x thin films. Acta Crystallographica Section E Structure Reports Online, 63 (11) doi:10.1107/s1600536807049033

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Reference TypeJournal (article/letter/editorial)
TitleAn N-bridged tritungsten compound for the chemical vapor deposition of WN x thin films
JournalActa Crystallographica Section E Structure Reports Online
AuthorsKoller, JürgenAuthor
McElwee-White, LisaAuthor
Abboud, Khalil A.Author
Year2007 (November 1)Volume63
Issue11
PublisherInternational Union of Crystallography (IUCr)
DOIdoi:10.1107/s1600536807049033Search in ResearchGate
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Mindat Ref. ID467030Long-form Identifiermindat:1:5:467030:2
GUID0
Full ReferenceKoller, Jürgen, McElwee-White, Lisa, Abboud, Khalil A. (2007) An N-bridged tritungsten compound for the chemical vapor deposition of WN x thin films. Acta Crystallographica Section E Structure Reports Online, 63 (11) doi:10.1107/s1600536807049033
Plain TextKoller, Jürgen, McElwee-White, Lisa, Abboud, Khalil A. (2007) An N-bridged tritungsten compound for the chemical vapor deposition of WN x thin films. Acta Crystallographica Section E Structure Reports Online, 63 (11) doi:10.1107/s1600536807049033
In(2007, November) Acta Crystallographica Section E Structure Reports Online Vol. 63 (11) International Union of Crystallography (IUCr)
Abstract/NotesIn the title compound, octachlorido-1κ4
Cl,3κ4
Cl-di-μ2-nitrido-1:2κ2
N:N;2:3κ2
N:N-tetrapyridine-1κN,2κ2
N,3κN-bis(trimethylsilylimido-2κN)tritungsten(V) dichloromethane disolvate, [W3(C3H9NSi)2Cl8N2(C5H5N)4]·2CH2Cl2, the central W metal atom is located on a twofold rotation axis and is coordinated in a distorted octahedral environment by two trimethylsilylimido groups, two pyridine molecules and two μ-N atoms which bridge it to the two other W atoms. These terminal W centers also show a distorted octahedral coordination, the bridging N atom and the pyridine ligand being trans with respect to each other. Additionally, four Cl atoms are bound to each terminal W atom, in a square-planar geometry, completing the octahedral coordination.


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