Curtis, Neil F., Waters, Joyce M., Rickard, Clifton E. (2001) [(1RS,4RS)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca-7,12-diene-N1,N4,N8,N12]nickel(II) diperchlorate. Acta Crystallographica Section E Structure Reports Online, 57 (1) doi:10.1107/s1600536800020559
| Reference Type | Journal (article/letter/editorial) | ||
|---|---|---|---|
| Title | [(1RS,4RS)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca-7,12-diene-N1,N4,N8,N12]nickel(II) diperchlorate | ||
| Journal | Acta Crystallographica Section E Structure Reports Online | ||
| Authors | Curtis, Neil F. | Author | |
| Waters, Joyce M. | Author | ||
| Rickard, Clifton E. | Author | ||
| Year | 2001 (January 1) | Volume | 57 |
| Issue | 1 | ||
| Publisher | International Union of Crystallography (IUCr) | ||
| DOI | doi:10.1107/s1600536800020559Search in ResearchGate | ||
| Generate Citation Formats | |||
| Mindat Ref. ID | 445451 | Long-form Identifier | mindat:1:5:445451:3 |
| GUID | 0 | ||
| Full Reference | Curtis, Neil F., Waters, Joyce M., Rickard, Clifton E. (2001) [(1RS,4RS)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca-7,12-diene-N1,N4,N8,N12]nickel(II) diperchlorate. Acta Crystallographica Section E Structure Reports Online, 57 (1) doi:10.1107/s1600536800020559 | ||
| Plain Text | Curtis, Neil F., Waters, Joyce M., Rickard, Clifton E. (2001) [(1RS,4RS)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca-7,12-diene-N1,N4,N8,N12]nickel(II) diperchlorate. Acta Crystallographica Section E Structure Reports Online, 57 (1) doi:10.1107/s1600536800020559 | ||
| In | (2001, January) Acta Crystallographica Section E Structure Reports Online Vol. 57 (1) International Union of Crystallography (IUCr) | ||
| Abstract/Notes | The title compound, [Ni(C17H34N4)](ClO4)2, has singlet ground-state nickel(II) complex cations in tetrahedrally twisted square-planar coordination by the four N atoms of the 15-membered diamine diimine tetraazamacrocycle and disordered perchlorate anions, linked into molecular clusters by N—H...O hydrogen bonds and weak Ni...O interactions. The cation has approximate twofold symmetry, with bond lengths Ni—Namineof 1.920 (2) and 1.924 (2) Å, and Ni—Nimineof 1.915 (2) and 1.929 (2) Å, andtrans–N—Ni—N angles of 165.1 (1) and 163.4 (1)°, with the shortest Ni...O distance being 3.27 (3) Å. | ||
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