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Identity HelpHelp with identification

3rd Apr 2021 19:56 UTCBecky Coulson 🌟 Expert

04663290017064863475210.jpg
Hello, I am helping a friend identify minerals for which labels are lost.  He has been able to do a streak test (dark grey to black) and has a set of hardness points (it's between 5 and 6).  He does not have a locality.
So...not galena, not hematite...skutterudite?  Suggestions appreciated.  I do not have the mineral, only photos so I am hoping they help.
Many thanks, Becky

3rd Apr 2021 20:00 UTCBecky Coulson 🌟 Expert

02833560017064863489645.jpg
Another view

3rd Apr 2021 20:01 UTCBecky Coulson 🌟 Expert

04181580017064863486622.jpg
another view - thanks!

3rd Apr 2021 20:47 UTCFrank K. Mazdab 🌟 Manager

Particularly from the last photo showing the uneven front face, it does look like a skutterudite, similar to the Moroccan ones. The hardness also matches. A density determination would additionally help, but it may not be possible (or practical or desired) to remove the specimen from its plastic base. Of course, doing a specific gravity measurement on the whole mass (mineral, base, and glue) might still be worthwhile and would set a lower limit, and may even approach that the mineral if there's a large density difference between the mineral and the plastic (presumably there is) and if also the mineral dominates the overall volume of the pair (maybe somewhat here).

3rd Apr 2021 21:54 UTCBecky Coulson 🌟 Expert

Thank you, Frank.  He does has a good electronic balance, so if he has a graduated container we might manage density eventually.  He is certainly determined in his efforts!

3rd Apr 2021 22:21 UTCFrank K. Mazdab 🌟 Manager

A graduated container actually isn't necessary, and in fact it's tougher to measure volume precisely than it is to measure mass or weight precisely. Weigh the sample on the electronic balance (Wmineral), then weigh a cup of water on the balance with a sufficient volume of water so later the sample can be fully immersed (Wtare), and then finally weigh the combination of the cup of water with the sample carefully suspended into it with a thin string or hair so it is fully submerged in the water and doesn't touch the bottom (Wsuspended).

The specific gravity is the weight of the mineral in air (= Wmineral) divided by the weight of the displaced volume of water (= [Wsuspended - Wtare]).

Or fully written out:

Wmineral / (Wsuspended - Wtare)

edit: oops... I initially had an extra Wmineral in there, but I think I got it right this time.

4th Apr 2021 07:07 UTCBecky Coulson 🌟 Expert

Thank you, Frank and Keith,
Frank, I forgot about using water with the mineral suspended - thanks!
Becky

4th Apr 2021 08:02 UTCFrank Mersch

The plastic base should not be a real problem: Volume can be calulated easily (V=l x w x h) and density of the poylmer will be 1.2 (PMMA or PC). That gives the mass of the base, too.

BR

Frank

4th Apr 2021 09:10 UTCFrank K. Mazdab 🌟 Manager

good point Frank. Adjusting the combined mineral+base measurements for the mass and volume of the base will require a few extra math steps, but it's certainly not difficult to calculate, and doing so should result in a fairly accurate SG estimate of the mineral.

4th Apr 2021 09:58 UTCFrank Mersch

Mass crystal = Mass Total - Mass base (calculated by measured rectanguar Volume)
Volume crystal = Volume total - Volume base

volume base = height x width x length (all in cm - I am a child of SI)
mass base = volume (in cm3) * 1.2g/cm3

Not that hard ;-)

BR + happy egg hunting

Frank

3rd Apr 2021 21:59 UTCKeith Compton 🌟 Manager

Very much looks like skutterudite from Morocco
 
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