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Nickenichite

A valid IMA mineral species
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02938200014977718468952.jpg
Nickenichite

Arsenatnaya fumarole, Second scoria cone, Northern Breakthrough, Great Fissure eruption, Tolbachik Volcanic field, Milkovsky District, Kamchatka Krai, Russia
03761550017068605203307.jpg
Nickenichite

Arsenatnaya fumarole, Second scoria cone, Northern Breakthrough, Great Fissure eruption, Tolbachik Volcanic field, Milkovsky District, Kamchatka Krai, Russia
09789900014948661133956.jpg
Nickenichite, etc.

Nickenichite-bearing fumarole, Nickenicher Sattel, Nickenich, Pellenz, Mayen-Koblenz, Rhineland-Palatinate, Germany
02938200014977718468952.jpg
Nickenichite

Arsenatnaya fumarole, Second scoria cone, Northern Breakthrough, Great Fissure eruption, Tolbachik Volcanic field, Milkovsky District, Kamchatka Krai, Russia
06621900017055319795667.jpg
Nickenichite

Arsenatnaya fumarole, Second scoria cone, Northern Breakthrough, Great Fissure eruption, Tolbachik Volcanic field, Milkovsky District, Kamchatka Krai, Russia
09789900014948661133956.jpg
Nickenichite, etc.

Nickenichite-bearing fumarole, Nickenicher Sattel, Nickenich, Pellenz, Mayen-Koblenz, Rhineland-Palatinate, Germany
02938200014977718468952.jpg
Nickenichite

Arsenatnaya fumarole, Second scoria cone, Northern Breakthrough, Great Fissure eruption, Tolbachik Volcanic field, Milkovsky District, Kamchatka Krai, Russia
05347330017068604527112.jpg
Nickenichite

Arsenatnaya fumarole, Second scoria cone, Northern Breakthrough, Great Fissure eruption, Tolbachik Volcanic field, Milkovsky District, Kamchatka Krai, Russia
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About NickenichiteHide

09001720016006014994955.jpg
View of the Nickenich lava quarrying, in 1910.

Nickenicher Sattel, Nickenich, Pellenz, Mayen-Koblenz, Rhineland-Palatinate, Germany
Formula:
Na0.8Ca0.4Cu0.4(Mg,Fe)3(AsO4)3
Colour:
Bright blue to gray blue.
Lustre:
Sub-Vitreous
Hardness:
3
Specific Gravity:
4.06 (Calculated)
Crystal System:
Monoclinic
Name:
Named by M. Auernhammer, H. Effenberger, G. Hentschel, Th. Reinecke, and E. Tillmanns in 1993 for the type locality at Nickenicher Sattel (Eicher Sattel), Eich, Andernach, Eifel Mts, Rhineland-Palatinate, Germany.
This page provides mineralogical data about Nickenichite.


Unique IdentifiersHide

Mindat ID:
2900
Long-form identifier:
mindat:1:1:2900:7
GUID
(UUID V4):
424a7646-5f2f-4861-ae58-68a2f1d63e19

IMA Classification of NickenichiteHide

Classification of NickenichiteHide

Strunz-mindat (2024):
8.AC.10

8 : PHOSPHATES, ARSENATES, VANADATES
A : Phosphates, etc. without additional anions, without H2O
C : With medium-sized and large cations
Dana 7th ed.:
38.2.7.3
Dana 8th ed.:
38.2.3.9

38 : ANHYDROUS NORMAL PHOSPHATES, ARSENATES, AND VANADATES
2 : (AB)5(XO4)3

Mineral SymbolsHide

As of 2021 there are now IMA–CNMNC approved mineral symbols (abbreviations) for each mineral species, useful for tables and diagrams.

SymbolSourceReference
NknIMA–CNMNCWarr, L.N. (2021). IMA–CNMNC approved mineral symbols. Mineralogical Magazine, 85(3), 291-320. doi:10.1180/mgm.2021.43

Physical Properties of NickenichiteHide

Lustre:
Sub-Vitreous
Transparency:
Translucent
Colour:
Bright blue to gray blue.
Hardness:
3 on Mohs scale
Tenacity:
Brittle
Cleavage:
Perfect
{010} perfect; {100} and {101} good.
Density:
4.06 g/cm3 (Calculated)

Optical Data of NickenichiteHide

Type:
Biaxial (+)
RI values:
nα = 1.714(5) nβ = 1.744(5) nγ = 1.783(5)
2V:
Measured: 60° to 84°, Calculated: 86°
Birefringence:
0.069
Max Birefringence:
δ = 0.069
Image shows birefringence interference colour range (at 30µm thickness)
and does not take into account mineral colouration.
Surface Relief:
High
Dispersion:
weak
Optical Extinction:
Z ∧ a = 28° on (010); Y = b.
Pleochroism:
Weak
Comments:
Light blue to blue.

Chemistry of NickenichiteHide

Mindat Formula:
Na0.8Ca0.4Cu0.4(Mg,Fe)3(AsO4)3
Elements listed:
As, Ca, Cu, Fe, Mg, Na, O - search for minerals with similar chemistry
Common Impurities:
K,Mn,P

Crystallography of NickenichiteHide

Crystal System:
Monoclinic
Class (H-M):
2/m - Prismatic
Space Group:
B2/b
Setting:
C2/c
Cell Parameters:
a = 11.882 Å, b = 12.76 Å, c = 6.647 Å
β = 112.81°
Ratio:
a:b:c = 0.931 : 1 : 0.521
Unit Cell V:
928.97 ų (Calculated from Unit Cell)
Z:
4
Morphology:
Fibrous to long prismatic. Elongate [101], commonly radial or lamellar parallel to (010), some showing {010}, {100}, and {101}.
Comment:
TMPM 48:153 (1993) structure.

Crystal StructureHide

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IDSpeciesReferenceLinkYearLocalityPressure (GPa)Temp (K)
0014632NickenichiteAuernhammer M, Effenberger H, Hentschel G, Reinecke T, Tillmanns E (1993) Nickenichite, a new arsenate from the Eifel, Germany Mineralogy and Petrology 48 153-1661993Nickenich, Nickenicher Sattel, Eifel, Germany0293
CIF Raw Data - click here to close

X-Ray Powder DiffractionHide

Powder Diffraction Data:
d-spacingIntensity
4.35 Å(40)
4.06 Å(50)
3.56 Å(40)
3.53 Å(40)
3.20 Å(60)
3.07 Å(40)
2.74 Å(100)
2.61 Å(40)
Comments:
TMPM 48:153 (1993)

Geological EnvironmentHide

Paragenetic Mode(s):
Paragenetic ModeEarliest Age (Ga)
Stage 7: Great Oxidation Event<2.4
45a : [Sulfates, arsenates, selenates, antimonates]

Type Occurrence of NickenichiteHide

Type Locality:
ⓘ Nickenichite-bearing fumarole, Nickenicher Sattel, Nickenich, Pellenz, Mayen-Koblenz, Rhineland-Palatinate, Germany
General Appearance of Type Material:
Bright blue fibrous to long prismatic monoclinic grains up to 0.20 mm long and 0.03 mm in diameter, elongate [101], commonly radial or lamellar parallel to (010).
Place of Conservation of Type Material:
University of Vienna, Vienna, Austria.
Geological Setting of Type Material:
Scoriaceous basalt from a Quaternary volcano.
Associated Minerals at Type Locality:
VanadiniteDuhamelite
Reference:
Auernhammer, M., Effenberger, H., Hentschel, G., Reinecke, Th. and Tillmanns, E. (1993): Nickenichite, a new arsenate from the Eifel, Germany. Mineralogy and Petrology, 48, 153-166.

Synonyms of NickenichiteHide

Other Language Names for NickenichiteHide

Relationship of Nickenichite to other SpeciesHide

Member of:
Alluaudite Group > Alluaudite Supergroup
Other Members of this group:
Alluaudite(Na,Ca)Mn2+(Fe3+,Mn2+,Fe2+,Mg)2(PO4)3Mon. 2/m : B2/b
Alluaudite-Ca□◻4Ca4Mn2+4Fe3+8(PO4)12Mon. 2/m : B2/b
Alluaudite-Na□◻4Na4Mn2+4Fe3+8(PO4)12Mon. 2/m : B2/b
ArseniopleiteNaCaMnMn2(AsO4)3Mon. 2/m
BadaloviteNa2Mg2Fe(AsO4)3Mon. 2/m : B2/b
BradaczekiteNaCu4(AsO4)3Mon. 2/m : B2/b
CalciohatertiteNaNaCa(CaFe3+)(AsO4)3Mon. 2/m : B2/b
CalciojohilleriteNaCaMg3(AsO4)3Mon. 2/m : B2/b
CamanchacaiteNaCaMg2[AsO4][AsO3(OH)]2Mon. 2/m : B2/b
CanutiteNaMn3[AsO4][AsO3(OH)]2Mon. 2/m : B2/b
Caryinite(Na,Pb)(Ca,Na)CaMn2+2(AsO4)3Mon. 2/m
ErikapohliteCu3(Zn,Cu,Mg)4Ca2(AsO4)6 · 2H2O Mon. 2/m : B2/m
Ferroalluaudite(Na,Ca)Fe2+(Fe3+,Mn2+,Fe2+)2(PO4)3Mon. 2/m : B2/b
Ferroalluaudite-NaNaNa4Na4Fe2+4Fe3+8(PO4)12Mon. 2/m : B2/m
FerrohagendorfiteNaCaFe2+Fe2+2(PO4)3Mon.
GroatiteNaCaMn2(PO4)[PO3(OH)]2Mon. 2/m : B2/b
HagendorfiteNaCaMn2+Fe2+2(PO4)3Mon. 2/m : B2/b
Hagendorfite-NaNaNaNaFe2+(Mn2+,Mn3+)(PO4)3 (?)Mon. 2/m : B2/b
HatertiteNa2(Ca,Na)(Fe3+,Cu)2(AsO4)3Mon. 2/m : B2/b
JohilleriteNa(Mg,Zn)3Cu(AsO4)3Mon. 2/m : B2/b
KeyiteCu2+3Zn4Cd2(AsO4)6 · 2H2OMon. 2/m
KhrenoviteNa3Fe3+2(AsO4)3Mon. 2/m : B2/b
Maghagendorfite(Na,◻)MgMn2+(Fe2+,Fe3+)2(PO4)3Mon. 2/m
MagnesiocanutiteNaMnMg2[AsO4]2[AsO2(OH)2]Mon. 2/m : B2/b
Magnesiohatertite(Na,Ca)2Ca(Mg,Fe3+)2(AsO4)3Mon. 2/m : B2/b
O'DanieliteNa(Zn,Mg)3(AsO4)(AsO3OH)2Mon. 2/m : B2/b
ParaberzeliiteNaCa2Mg2(AsO4)3Mon. 2/m : B2/b
Unnamed (Na-Mg Arsenate Hydroxyarsenate)NaMg3(AsO4)(AsO3OH)2Mon. 2/m : B2/b
Unnamed (Na-Zn-H Arsenate Hydrxyarsenate)Na(Na0.6Zn0.4)Zn2(H0.6AsO4)(AsO3OH)2Mon. 2/m : B2/b
VaruliteNaCaMn2+Mn2+2(PO4)3Mon. 2/m : B2/b
YazganiteNaFe3+2(Mg,Mn2+)(AsO4)3 · H2OMon. 2/m : B2/b
ZhanghuifeniteNa3Mn4Mg2Al(PO4)6Mon. 2/m
ZincobradaczekiteNaZn2Cu2(AsO4)3Mon. 2/m : B2/b

Common AssociatesHide

Associated Minerals Based on Photo Data:
17 photos of Nickenichite associated with VanadinitePb5(VO4)3Cl
1 photo of Nickenichite associated with OrthoclaseK(AlSi3O8)
1 photo of Nickenichite associated with HematiteFe2O3
1 photo of Nickenichite associated with TenoriteCuO

Related Minerals - Strunz-mindat GroupingHide

8.AC.AngarfiteNaFe3+5(PO4)4(OH)4 · 4H2O Orth. 2 2 2 : C2 2 21
8.AC.WopmayiteCa6Na3◻Mn(PO4)3(PO3OH)4 Trig. 3m : R3c
8.AC.XDyrnaesite-(La)Na8Ce4+(La,REE)2(PO4)6Orth. mmm (2/m 2/m 2/m) : Pnma
8.AC.EdtolliteK2NaCu5Fe3+O2(AsO4)4Tric. 1 : P1
8.AC.AlumoedtolliteK2NaCu5AlO2(AsO4)4Tric. 1 : P1
8.AC.CrocobeloniteCaFe3+2O(PO4)2Orth. mmm (2/m 2/m 2/m) : Pnma
8.AC.ManganobadaloviteNaNaMn(MgFe3+)(AsO4)3Mon. 2/m : B2/b
8.AC.BeershevaiteCaFe3+3(PO4)3OMon. 2/m : P21/m
8.AC.CalciohatertiteNaNaCa(CaFe3+)(AsO4)3Mon. 2/m : B2/b
8.AC.KabaloviteFe2+3Fe3+4(PO4)6Tric. 1 : P1
8.AC.Nazarchukite Ca2NiFe3+2(PO4)4Orth. mmm (2/m 2/m 2/m) : Pbca
8.AC.Changesite–(Y)(Ca8Y)◻Fe2+(PO4)7Trig. 3m : R3c
8.AC.Crocobelonite-1MCaFe3+2O(PO4)2Mon. 2/m : P21/m
8.AC.Ebnerite(NH4)Zn(PO4)Hex. 6 : P63
8.AC.MagnesioqingheiiteNa2Mg(MgAl)(PO4)3Mon. 2/m
8.AC.Epiebnerite(NH4)Zn(PO4)Mon. 2 : P21
8.AC.02GrigorieviteCu3Fe3+2Al2(VO4)6Tric. 1 : P1
8.AC.02KoksharoviteCaMg2Fe3+4(VO4)6Tric. 1 : P1
8.AC.02ZiminaiteFe3+ 6 (VO4)6Tric. 1 : P1
8.AC.05CalciojohilleriteNaCaMg3(AsO4)3Mon. 2/m : B2/b
8.AC.05HowardevansiteNaCuFe2(VO4)3Tric. 1 : P1
8.AC.05O'DanieliteNa(Zn,Mg)3(AsO4)(AsO3OH)2Mon. 2/m : B2/b
8.AC.05 vaAlluaudite-Na□◻4Na4Mn2+4Fe3+8(PO4)12Mon. 2/m : B2/b
8.AC.05 vaAlluaudite-Ca□◻4Ca4Mn2+4Fe3+8(PO4)12Mon. 2/m : B2/b
8.AC.05 vaFerroalluaudite-NaNaNa4Na4Fe2+4Fe3+8(PO4)12Mon. 2/m : B2/m
8.AC.05Hagendorfite-NaNaNaNaFe2+(Mn2+,Mn3+)(PO4)3 (?)Mon. 2/m : B2/b
8.AC.05ErikapohliteCu3(Zn,Cu,Mg)4Ca2(AsO4)6 · 2H2O Mon. 2/m : B2/m
8.AC.05HatertiteNa2(Ca,Na)(Fe3+,Cu)2(AsO4)3Mon. 2/m : B2/b
8.AC.05Unnamed (Na-Mg Arsenate Hydroxyarsenate)NaMg3(AsO4)(AsO3OH)2Mon. 2/m : B2/b
8.AC.05Unnamed (Na-Zn-H Arsenate Hydrxyarsenate)Na(Na0.6Zn0.4)Zn2(H0.6AsO4)(AsO3OH)2Mon. 2/m : B2/b
8.AC.05ZincobradaczekiteNaZn2Cu2(AsO4)3Mon. 2/m : B2/b
8.AC.05BadaloviteNa2Mg2Fe(AsO4)3Mon. 2/m : B2/b
8.AC.05MagnesiocanutiteNaMnMg2[AsO4]2[AsO2(OH)2]Mon. 2/m : B2/b
8.AC.05Magnesiohatertite(Na,Ca)2Ca(Mg,Fe3+)2(AsO4)3Mon. 2/m : B2/b
8.AC.05KhrenoviteNa3Fe3+2(AsO4)3Mon. 2/m : B2/b
8.AC.05ParaberzeliiteNaCa2Mg2(AsO4)3Mon. 2/m : B2/b
8.AC.05CamanchacaiteNaCaMg2[AsO4][AsO3(OH)]2Mon. 2/m : B2/b
8.AC.05ManganohatertiteNaNaCa(MnFe3+)(AsO4)3Mon. 2/m : B2/b
8.AC.07ZhanghuifeniteNa3Mn4Mg2Al(PO4)6Mon. 2/m
8.AC.07FerrobobfergusoniteNa2Fe2+5Fe3+Al(PO4)6Mon.
8.AC.10Alluaudite(Na,Ca)Mn2+(Fe3+,Mn2+,Fe2+,Mg)2(PO4)3Mon. 2/m : B2/b
8.AC.10ArseniopleiteNaCaMnMn2(AsO4)3Mon. 2/m
8.AC.10Caryinite(Na,Pb)(Ca,Na)CaMn2+2(AsO4)3Mon. 2/m
8.AC.10Ferroalluaudite(Na,Ca)Fe2+(Fe3+,Mn2+,Fe2+)2(PO4)3Mon. 2/m : B2/b
8.AC.10HagendorfiteNaCaMn2+Fe2+2(PO4)3Mon. 2/m : B2/b
8.AC.10JohilleriteNa(Mg,Zn)3Cu(AsO4)3Mon. 2/m : B2/b
8.AC.10Maghagendorfite(Na,◻)MgMn2+(Fe2+,Fe3+)2(PO4)3Mon. 2/m
8.AC.10VaruliteNaCaMn2+Mn2+2(PO4)3Mon. 2/m : B2/b
8.AC.10FerrohagendorfiteNaCaFe2+Fe2+2(PO4)3Mon.
8.AC.10BradaczekiteNaCu4(AsO4)3Mon. 2/m : B2/b
8.AC.10GroatiteNaCaMn2(PO4)[PO3(OH)]2Mon. 2/m : B2/b
8.AC.15BobfergusoniteNa2Mn5FeAl(PO4)6Mon. 2/m : P2/b
8.AC.15Ferrowyllieite(Na,Ca,Mn)(Fe,Mn)(Fe,Fe,Mg)Al(PO4)3Mon. 2/m : P21/b
8.AC.15QingheiiteNaNaMn2+(MgAl)(PO4)3Mon. 2/m : P21/b
8.AC.15Rosemaryite(Na,Ca,Mn)(Mn,Fe2+)(Fe3+,Mg)Al(PO4)3Mon. 2/m : P21/b
8.AC.15Wyllieite(Na,Ca,Mn)(Mn,Fe)(Fe,Mg)Al(PO4)3Mon. 2/m
8.AC.15Ferrorosemaryite◻NaFe2+Fe3+Al(PO4)3Mon. 2/m
8.AC.15FerroqingheiiteNaNaFe2+(MgAl)(PO4)3Mon. 2/m : P21/m
8.AC.17CzochralskiiteNa4Ca3Mg(PO4)4Orth. mmm (2/m 2/m 2/m) : Pnma
8.AC.18ManitobaiteNa16Mn2+ 25Al8(PO4)30Mon. m : Pb
8.AC.20MarićiteNaFe2+(PO4)Orth. mmm (2/m 2/m 2/m) : Pmna
8.AC.25Berzeliite(NaCa2)Mg2(AsO4)3Iso. m3m (4/m 3 2/m) : Ia3d
8.AC.25Manganberzeliite(NaCa2)Mn2+2(AsO4)3Iso. m3m (4/m 3 2/m) : Ia3d
8.AC.25Palenzonaite(NaCa2)Mn2+2(VO4)3Iso. m3m (4/m 3 2/m) : Ia3d
8.AC.25Schäferite(NaCa2)Mg2(VO4)3Iso. m3m (4/m 3 2/m) : Ia3d
8.AC.25Hedegaardite(Ca,Na)9(Ca,Na)Mg(PO4)6(PO3OH)Trig. 3m : R3c
8.AC.25MatyhiteCa18(Ca,◻)2Fe2+2(PO4)14Trig. 3m : R3c
8.AC.30BrianiteNa2CaMg(PO4)2Mon. 2/m : P21/b
8.AC.35Vitusite-(Ce)Na3(Ce,La,Nd)(PO4)2Orth. mm2 : Pca21
8.AC.40Olgite(Sr,Ba)(Na,Sr,REE)2Na(PO4)2Trig. 3m (3 2/m) : P3m1
8.AC.40Bario-olgite(Ba,Sr)(Na,Sr,REE)2Na(PO4)2 · Trig. 3 : P3
8.AC.45StrontiowhitlockiteSr9Mg(PO4)6(PO3OH)Trig. 3m : R3c
8.AC.45WhitlockiteCa9Mg(PO4)6(PO3OH)Trig. 3m : R3c
8.AC.45MerrilliteCa9NaMg(PO4)7Trig. 3m : R3m
8.AC.45TuiteCa3(PO4)2Trig. 3m (3 2/m) : R3m
8.AC.45FerromerrilliteCa9NaFe2+(PO4)7Trig. 3m : R3c
8.AC.47IwateiteNa2BaMn(PO4)2Trig. 3 : P3
8.AC.47YurmariniteNa7(Fe3+,Mg,Cu)4(AsO4)6Trig. 3m (3 2/m) : R3c
8.AC.47OzerovaiteNa2KAl3(AsO4)4Orth. mmm (2/m 2/m 2/m) : Cmca
8.AC.47AnatolyiteNa6(Ca,Na)(Mg,Fe3+)3Al(AsO4)6Trig. 3m (3 2/m) : R3c
8.AC.47PansneriteK3Na3(Fe3+,Al)6(AsO4)8Orth. mmm (2/m 2/m 2/m)
8.AC.50ChladniiteNa3CaMg11(PO4)9Trig. 3 : R3
8.AC.50FillowiteNa3CaMn2+11(PO4)9Trig. 3 : R3
8.AC.50JohnsomervilleiteNa3CaFe11(PO4)9Trig. 3 : R3
8.AC.50GalileiiteNa3Fe2+Fe2+11(PO4)9Trig. 3 : R3
8.AC.50XenophylliteNa4Fe2+7(PO4)6Tric. 1 : P1
8.AC.50UdinaiteNaMg4(VO4)3Tet. 4 2m : I4 2d
8.AC.50ArsenudinaiteNaMg4(AsO4)3Tet. 4 2m : I4 2d
8.AC.52Lasnierite(Ca,Sr)(Mg,Fe2+)2Al(P[O,F]4)3Orth. mmm (2/m 2/m 2/m) : Pbcn
8.AC.55PharmazinciteKZnAsO4Hex. 6 : P63
8.AC.57ZubkovaiteCa3Cu3(AsO4)4Mon. 2 : B2
8.AC.60KosnariteKZr2(PO4)3Trig. 3m (3 2/m) : R3c
8.AC.65Panethite(Na,Ca)2(Mg,Fe2+)2(PO4)2Mon. 2/m : P21/b
8.AC.70StanfielditeCa4Mg5(PO4)6Mon.
8.AC.75RonneburgiteK2MnV4O12Mon. 2/m
8.AC.80TillmannsiteAg3Hg[(V,As)O4]Tet. 4 : I4
8.AC.85FilatoviteK(Al,Zn)2(As,Si)2O8Mon. 2/m

Fluorescence of NickenichiteHide

In UV light:
Not fluorescent.

Other InformationHide

Health Risks:
No information on health risks for this material has been entered into the database. You should always treat mineral specimens with care.

Internet Links for NickenichiteHide

References for NickenichiteHide

Localities for NickenichiteHide

This map shows a selection of localities that have latitude and longitude coordinates recorded. Click on the symbol to view information about a locality. The symbol next to localities in the list can be used to jump to that position on the map.

Locality ListHide

- This locality has map coordinates listed. - This locality has estimated coordinates. ⓘ - Click for references and further information on this occurrence. ? - Indicates mineral may be doubtful at this locality. - Good crystals or important locality for species. - World class for species or very significant. (TL) - Type Locality for a valid mineral species. (FRL) - First Recorded Locality for everything else (eg varieties). Struck out - Mineral was erroneously reported from this locality. Faded * - Never found at this locality but inferred to have existed at some point in the past (e.g. from pseudomorphs).

All localities listed without proper references should be considered as questionable.
Germany (TL)
 
  • Rhineland-Palatinate
    • Mayen-Koblenz
      • Pellenz
        • Nickenich
          • Nickenicher Sattel
Auernhammer et al. (1993)
Blass et al. (2006)
Italy
 
  • Campania
    • Naples
      • Somma-Vesuvius Complex
        • Mount Vesuvius
Russo et al. (2022)
Russia
 
  • Kamchatka Krai
    • Milkovsky District
      • Tolbachik Volcanic field
        • Great Fissure eruption (Main Fracture)
          • Northern Breakthrough (North Breach)
            • Second scoria cone
Stephan Wolfsried collection (from material analysed by Igor Pekov) +1 other reference
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